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A critical evaluation of the microstructural gradient along the build direction in electron beam melted Ti-6Al-4V alloy

A critical evaluation of the microstructural gradient along the build direction in electron beam melted Ti-6Al-4V alloy
A critical evaluation of the microstructural gradient along the build direction in electron beam melted Ti-6Al-4V alloy
It is generally recognised that electron beam melted (EBM) Ti-6Al-4V alloys exhibit a microstructural gradient along the build direction, but there have been some inconsistent experimental observations and debate as to the origin and magnitude of this effect. Here we present an unambiguous evaluation of this microstructural gradient and associated mechanical property along the EBM build direction on purpose-built round bar RB samples with build height of 380 mm and rectangular plate RP samples with build height of 120 mm. Columnar prior β grain width was found to increase (from 86 ± 38 to 154 ± 56 µm in RB and from 79 ± 34 to 122 ± 56 µm in RP samples) with the build height and the similar increase was also observed for α lath width (from 0.58 ± 24 to 0.87 ± 33 µm in RB and from 1.50 ± 45 to 1.80 ± 49 µm in RP samples). These observations can be attributed to the thermal gradient in the powder bed that produced a cooling rate gradient along the build height. The measured α lath width variation along the build height followed a log-normal distribution. The graded microstructure resulted in a decrease in micro-hardness which correlated very well with the mean α lath width by following a Hall-Petch relation.
0921-5093
182-194
Sharma, H.
02ca354d-3d07-42b4-b060-555c3985a18e
Parfitt, D.
b3490a0a-78a3-49ff-ac4c-ce83e02a0e6a
Syed, A.K.
55c97988-4b79-4e09-8c62-8a2daf07e837
Wimpenny, D.
c77d2c92-329d-485a-951a-1e70aaf4c1f0
Muzangaza, E.
6043bbd1-61d5-4cb0-82c6-84a01bf148bb
Baxter, G.
96260719-c9c6-4f7c-b51e-8f0a024a56e3
Chen, B.
be54a9a8-da2a-4e6f-ae0e-0b076be87daf
et al.
Sharma, H.
02ca354d-3d07-42b4-b060-555c3985a18e
Parfitt, D.
b3490a0a-78a3-49ff-ac4c-ce83e02a0e6a
Syed, A.K.
55c97988-4b79-4e09-8c62-8a2daf07e837
Wimpenny, D.
c77d2c92-329d-485a-951a-1e70aaf4c1f0
Muzangaza, E.
6043bbd1-61d5-4cb0-82c6-84a01bf148bb
Baxter, G.
96260719-c9c6-4f7c-b51e-8f0a024a56e3
Chen, B.
be54a9a8-da2a-4e6f-ae0e-0b076be87daf

Sharma, H., Parfitt, D. and Syed, A.K. , et al. (2019) A critical evaluation of the microstructural gradient along the build direction in electron beam melted Ti-6Al-4V alloy. Materials Science and Engineering: A, 744, 182-194. (doi:10.1016/j.msea.2018.12.016).

Record type: Article

Abstract

It is generally recognised that electron beam melted (EBM) Ti-6Al-4V alloys exhibit a microstructural gradient along the build direction, but there have been some inconsistent experimental observations and debate as to the origin and magnitude of this effect. Here we present an unambiguous evaluation of this microstructural gradient and associated mechanical property along the EBM build direction on purpose-built round bar RB samples with build height of 380 mm and rectangular plate RP samples with build height of 120 mm. Columnar prior β grain width was found to increase (from 86 ± 38 to 154 ± 56 µm in RB and from 79 ± 34 to 122 ± 56 µm in RP samples) with the build height and the similar increase was also observed for α lath width (from 0.58 ± 24 to 0.87 ± 33 µm in RB and from 1.50 ± 45 to 1.80 ± 49 µm in RP samples). These observations can be attributed to the thermal gradient in the powder bed that produced a cooling rate gradient along the build height. The measured α lath width variation along the build height followed a log-normal distribution. The graded microstructure resulted in a decrease in micro-hardness which correlated very well with the mean α lath width by following a Hall-Petch relation.

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Accepted/In Press date: 4 December 2018
e-pub ahead of print date: 5 December 2018
Published date: 11 December 2019

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Local EPrints ID: 489945
URI: http://eprints.soton.ac.uk/id/eprint/489945
ISSN: 0921-5093
PURE UUID: 346866de-6848-4e93-a65c-28475399fadb
ORCID for B. Chen: ORCID iD orcid.org/0000-0003-1960-080X

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Date deposited: 08 May 2024 16:30
Last modified: 09 May 2024 04:01

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Contributors

Author: H. Sharma
Author: D. Parfitt
Author: A.K. Syed
Author: D. Wimpenny
Author: E. Muzangaza
Author: G. Baxter
Author: B. Chen ORCID iD
Corporate Author: et al.

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