Crystal structure of 4,4′-(disulfanediyl) dipyridinium chloride triiodide
Crystal structure of 4,4′-(disulfanediyl) dipyridinium chloride triiodide
4,4′-(Disulfanediyl)dipyridinium chloride triiodide, C10H10N2S2 2+·Cl-·I3 -, (1) was synthesized by reaction of 4,4′-dipyridyldisulfide with ICl in a 1:1 molar ratio in dichloromethane solution. The structural characterization of 1 by SC-XRD analysis was supported by elemental analysis, FT-IR, and FT-Raman spectroscopic measurements.
bis(pyridine-4-yl)disulfide, crystal structure, halogen bonding, polyhalides, polypyridyl donors, SC-XRD
641-644
Podda, Enrico
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Aragoni, M. Carla
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Caltagirone, Claudia
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De Filippo, Greta
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Garau, Alessandra
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Lippolis, Vito
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Mancini, Annalisa
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Pintus, Anna
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Orton, James B.
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Coles, Simon J.
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Arca, Massimiliano
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June 2024
Podda, Enrico
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Aragoni, M. Carla
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Caltagirone, Claudia
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De Filippo, Greta
75e7f402-a985-423b-8d31-12ddbc51f39f
Garau, Alessandra
0dbe375e-901e-4003-9700-45926d87a771
Lippolis, Vito
d9833a14-4aab-4827-a2ba-be818871dcf5
Mancini, Annalisa
da134433-ee68-449c-9d2f-cad90b37a553
Pintus, Anna
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Orton, James B.
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Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Arca, Massimiliano
f90b59f6-4dfb-471d-912e-3515e6507165
Podda, Enrico, Aragoni, M. Carla, Caltagirone, Claudia, De Filippo, Greta, Garau, Alessandra, Lippolis, Vito, Mancini, Annalisa, Pintus, Anna, Orton, James B., Coles, Simon J. and Arca, Massimiliano
(2024)
Crystal structure of 4,4′-(disulfanediyl) dipyridinium chloride triiodide.
Acta Crystallographica Section E: Crystallographic Communications, 80 (Part 6), .
(doi:10.1107/S2056989024004213).
Abstract
4,4′-(Disulfanediyl)dipyridinium chloride triiodide, C10H10N2S2 2+·Cl-·I3 -, (1) was synthesized by reaction of 4,4′-dipyridyldisulfide with ICl in a 1:1 molar ratio in dichloromethane solution. The structural characterization of 1 by SC-XRD analysis was supported by elemental analysis, FT-IR, and FT-Raman spectroscopic measurements.
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Accepted/In Press date: 7 May 2024
Published date: June 2024
Keywords:
bis(pyridine-4-yl)disulfide, crystal structure, halogen bonding, polyhalides, polypyridyl donors, SC-XRD
Identifiers
Local EPrints ID: 491851
URI: http://eprints.soton.ac.uk/id/eprint/491851
ISSN: 2056-9890
PURE UUID: c56ef1c1-bd89-4dac-827c-3d4bdf3cea0d
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Date deposited: 04 Jul 2024 17:12
Last modified: 12 Jul 2024 01:38
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Contributors
Author:
Enrico Podda
Author:
M. Carla Aragoni
Author:
Claudia Caltagirone
Author:
Greta De Filippo
Author:
Alessandra Garau
Author:
Vito Lippolis
Author:
Annalisa Mancini
Author:
Anna Pintus
Author:
James B. Orton
Author:
Massimiliano Arca
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