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Electrochemical reduction of C02 at multi-metallic interfaces

Electrochemical reduction of C02 at multi-metallic interfaces
Electrochemical reduction of C02 at multi-metallic interfaces

Oxide-derived (OD) Sn-Pb-Sb, and Cu-Sn alloy catalysts were prepared for electrochemical reduction of CO2 (eCO2R) for formate (HCOO-) and carbon monoxide (CO) production. The morphology, elemental mapping, and electrochemical behavior of the electrocatalysts were probed systematically. The results demonstrate that OD-Sn-Pb-Sb alloy improved the FEHCCO-remarkably from 68% to 91% without any reduction in current density. For eCO2R to CO production, Cu-Sn alloy electrodes were prepared and the results show that Cu-Sn alloy electrode reduces C02 to CO selectively (FE∼91%) at a high current density. The improved eCO2R performance of OD-Sn-Pb-Sb and Cu-Sn electrodes relative to their pristine electrodes could be attributed to local geometric and electronic structural changes.

1938-6737
10
57-66
Electrochemical Society Inc.
Rasul, Shahid
482cda2a-0a01-4f15-846a-c4aa2f73b824
Pugnant, Adrien
e67fc96f-94af-4530-a688-81e6a4cc64d6
Yu, Eileen H.
28e47863-4b50-4821-b80b-71fb5a2edef2
Staser, J. A.
Brisard, G.
Flake, J.
Mustain, W.
Zhou, X.-D.
Gur, T.
Mogensen, M.
Xu, H.
Rasul, Shahid
482cda2a-0a01-4f15-846a-c4aa2f73b824
Pugnant, Adrien
e67fc96f-94af-4530-a688-81e6a4cc64d6
Yu, Eileen H.
28e47863-4b50-4821-b80b-71fb5a2edef2
Staser, J. A.
Brisard, G.
Flake, J.
Mustain, W.
Zhou, X.-D.
Gur, T.
Mogensen, M.
Xu, H.

Rasul, Shahid, Pugnant, Adrien and Yu, Eileen H. (2018) Electrochemical reduction of C02 at multi-metallic interfaces. Staser, J. A., Brisard, G., Flake, J., Mustain, W., Zhou, X.-D., Gur, T., Mogensen, M. and Xu, H. (eds.) In ECS Transactions. vol. 85, Electrochemical Society Inc. pp. 57-66 . (doi:10.1149/08510.0057ecst).

Record type: Conference or Workshop Item (Paper)

Abstract

Oxide-derived (OD) Sn-Pb-Sb, and Cu-Sn alloy catalysts were prepared for electrochemical reduction of CO2 (eCO2R) for formate (HCOO-) and carbon monoxide (CO) production. The morphology, elemental mapping, and electrochemical behavior of the electrocatalysts were probed systematically. The results demonstrate that OD-Sn-Pb-Sb alloy improved the FEHCCO-remarkably from 68% to 91% without any reduction in current density. For eCO2R to CO production, Cu-Sn alloy electrodes were prepared and the results show that Cu-Sn alloy electrode reduces C02 to CO selectively (FE∼91%) at a high current density. The improved eCO2R performance of OD-Sn-Pb-Sb and Cu-Sn electrodes relative to their pristine electrodes could be attributed to local geometric and electronic structural changes.

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More information

Published date: 2018
Additional Information: Publisher Copyright: © The Electrochemical Society.
Venue - Dates: Symposium on Electrosynthesis of Fuels 5 - 233rd ECS Meeting, , Seattle, United States, 2018-05-13 - 2018-05-17

Identifiers

Local EPrints ID: 498612
URI: http://eprints.soton.ac.uk/id/eprint/498612
ISSN: 1938-6737
PURE UUID: 155b2560-fa34-44e1-9219-ea1fd67cf2f9
ORCID for Eileen H. Yu: ORCID iD orcid.org/0000-0002-6872-975X

Catalogue record

Date deposited: 24 Feb 2025 17:39
Last modified: 25 Feb 2025 03:14

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Contributors

Author: Shahid Rasul
Author: Adrien Pugnant
Author: Eileen H. Yu ORCID iD
Editor: J. A. Staser
Editor: G. Brisard
Editor: J. Flake
Editor: W. Mustain
Editor: X.-D. Zhou
Editor: T. Gur
Editor: M. Mogensen
Editor: H. Xu

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