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3D nanowire Pt catalysts with enhanced stability for the oxygen reduction reaction

3D nanowire Pt catalysts with enhanced stability for the oxygen reduction reaction
3D nanowire Pt catalysts with enhanced stability for the oxygen reduction reaction

We report that self-supporting mesoporous platinum 3D nanowires with a single diamond (SD) morphology and a high specific surface area of 40.4 m2 g-1 demonstrated enhanced stability toward the oxygen reduction reaction (ORR). These were found to be superior to commercially available carbon-supported Pt nanoparticles (Pt/C). After 1000 potential cycles, there was a 21% loss in surface area for SD-Pt, as compared with a 40.3% loss for Pt/C with no reduction in their half-wave potential (measured at J = 3.0 mA cm-2), whereas the Pt/C catalyst showed a 11.9 mV decrease. Our findings revealed that our SD-Pt thin films also exhibited excellent ORR activity, which offers significant potential for their application as high-performance cathode materials in alkaline fuel cells.

2470-1343
8082-8088
White, Joshua S.
3025791c-ba86-4207-8059-19ff2617122c
Liu, Wanli
ab42521f-970b-47f9-9dd4-7adb405331e4
Perry, Samuel C.
8e204d86-4a9c-4a5d-9932-cf470174648e
Akbar, Samina
161851df-f691-49ef-960c-c2f325c98357
Alba-Venero, Diego
5e2f071d-e58e-4d83-bf35-15fcb634788b
Terrill, Nicholas J.
e8e88533-2dd5-42f6-bb32-c25034e08a83
Squires, Adam
dcf51695-9a96-48aa-acf9-b76d0ab27e9b
Nandhakumar, Iris
e9850fe5-1152-4df8-8a26-ed44b5564b04
White, Joshua S.
3025791c-ba86-4207-8059-19ff2617122c
Liu, Wanli
ab42521f-970b-47f9-9dd4-7adb405331e4
Perry, Samuel C.
8e204d86-4a9c-4a5d-9932-cf470174648e
Akbar, Samina
161851df-f691-49ef-960c-c2f325c98357
Alba-Venero, Diego
5e2f071d-e58e-4d83-bf35-15fcb634788b
Terrill, Nicholas J.
e8e88533-2dd5-42f6-bb32-c25034e08a83
Squires, Adam
dcf51695-9a96-48aa-acf9-b76d0ab27e9b
Nandhakumar, Iris
e9850fe5-1152-4df8-8a26-ed44b5564b04

White, Joshua S., Liu, Wanli, Perry, Samuel C., Akbar, Samina, Alba-Venero, Diego, Terrill, Nicholas J., Squires, Adam and Nandhakumar, Iris (2025) 3D nanowire Pt catalysts with enhanced stability for the oxygen reduction reaction. ACS Omega, 10 (8), 8082-8088. (doi:10.1021/acsomega.4c06385).

Record type: Article

Abstract

We report that self-supporting mesoporous platinum 3D nanowires with a single diamond (SD) morphology and a high specific surface area of 40.4 m2 g-1 demonstrated enhanced stability toward the oxygen reduction reaction (ORR). These were found to be superior to commercially available carbon-supported Pt nanoparticles (Pt/C). After 1000 potential cycles, there was a 21% loss in surface area for SD-Pt, as compared with a 40.3% loss for Pt/C with no reduction in their half-wave potential (measured at J = 3.0 mA cm-2), whereas the Pt/C catalyst showed a 11.9 mV decrease. Our findings revealed that our SD-Pt thin films also exhibited excellent ORR activity, which offers significant potential for their application as high-performance cathode materials in alkaline fuel cells.

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Accepted/In Press date: 10 February 2025
e-pub ahead of print date: 21 February 2025
Published date: 4 March 2025

Identifiers

Local EPrints ID: 499491
URI: http://eprints.soton.ac.uk/id/eprint/499491
ISSN: 2470-1343
PURE UUID: 1bad8a98-c5d2-46e7-a8ea-6067636a4bc6
ORCID for Samuel C. Perry: ORCID iD orcid.org/0000-0002-6263-6114
ORCID for Samina Akbar: ORCID iD orcid.org/0000-0002-9456-3861
ORCID for Iris Nandhakumar: ORCID iD orcid.org/0000-0002-9668-9126

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Date deposited: 21 Mar 2025 17:47
Last modified: 22 Aug 2025 02:39

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Contributors

Author: Joshua S. White
Author: Wanli Liu
Author: Samuel C. Perry ORCID iD
Author: Samina Akbar ORCID iD
Author: Diego Alba-Venero
Author: Nicholas J. Terrill
Author: Adam Squires

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