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Anisotropic Ta2O5 photonic crystal waveguide etching using inductively coupled plasma etching

Anisotropic Ta2O5 photonic crystal waveguide etching using inductively coupled plasma etching
Anisotropic Ta2O5 photonic crystal waveguide etching using inductively coupled plasma etching

Achieving smooth and vertical sidewall profile in the 2D photonic crystals (PhCs) is crucial for the photonic crystal waveguides (PCWs) in integrated optical devices, since “volcano” shaped PhCs lead to light leakage and the drift of photonic bandgap. This paper optimizes the inductively coupled plasma reactive ion etching (ICP-RIE) process for improving the sidewall profile of Ta 2 O 5 PCW with minimum PhC dimension of 300 nm pitch and 185 nm diameter. A set of experiments was generated by statistical software (minitab) to efficiently investigate the region of interest in the process space by varying RF platen power, ICP power, % C 4 F 8 in gas mixture ( C 4 F 8 and O 2 ), and chamber pressure. Subsequently, the most suitable experimental conditions were identified and used as the central run for analyzing the influence of individual parameters on ICP etching of Ta 2 O 5 . Key findings include the importance of maintaining a 50% C 4 F 8 in total gas flow and trade-offs related to ICP and RF power adjustments. Pressure has a negligible impact on sidewall angle but exerts a more pronounced influence on etch rate and micromasking. A delicate balance among these parameters is crucial for optimal etching results. The recommended recipe (50 W RF platen power, 2000 W ICP power, 10 mTorr pressure, 50% C 4 F 8 in total gas flow) achieves an etch rate of 113.325 nm/min with a smooth and vertical sidewall in PhCs. The entire etching exploration process was conducted on a Ta 2 O 5 layer deposited on a Si substrate. Additionally, this recipe was applied to etch Ta 2 O 5 with a 2 μ m SiO 2 layer interposed between the Ta 2 O 5 layer and the Si substrate, yielding favorable results and preserving the integrity of the PhC sidewall.

Wang, Wenjie
f06ced2c-bc2f-4816-92cf-f0ad49f63565
Arzubiaga Totorika, Libe
a9f933d1-6768-4ca4-b5c5-fa68797ae548
Shayesteh, Maryam
660d4bbc-ec8a-4cde-81d7-4f0f5f61bb98
Fenner, Stephen Stapleton
a01d73ed-e4b7-47b8-9982-c2f361588481
Clark, Owain
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Charlton, Martin
fcf86ab0-8f34-411a-b576-4f684e51e274
Wang, Wenjie
f06ced2c-bc2f-4816-92cf-f0ad49f63565
Arzubiaga Totorika, Libe
a9f933d1-6768-4ca4-b5c5-fa68797ae548
Shayesteh, Maryam
660d4bbc-ec8a-4cde-81d7-4f0f5f61bb98
Fenner, Stephen Stapleton
a01d73ed-e4b7-47b8-9982-c2f361588481
Clark, Owain
d2b922ab-3d98-42fc-97d9-042644666f73
Charlton, Martin
fcf86ab0-8f34-411a-b576-4f684e51e274

Wang, Wenjie, Arzubiaga Totorika, Libe, Shayesteh, Maryam, Fenner, Stephen Stapleton, Clark, Owain and Charlton, Martin (2025) Anisotropic Ta2O5 photonic crystal waveguide etching using inductively coupled plasma etching. Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, 43 (2), [023405]. (doi:10.1116/6.0004211).

Record type: Article

Abstract

Achieving smooth and vertical sidewall profile in the 2D photonic crystals (PhCs) is crucial for the photonic crystal waveguides (PCWs) in integrated optical devices, since “volcano” shaped PhCs lead to light leakage and the drift of photonic bandgap. This paper optimizes the inductively coupled plasma reactive ion etching (ICP-RIE) process for improving the sidewall profile of Ta 2 O 5 PCW with minimum PhC dimension of 300 nm pitch and 185 nm diameter. A set of experiments was generated by statistical software (minitab) to efficiently investigate the region of interest in the process space by varying RF platen power, ICP power, % C 4 F 8 in gas mixture ( C 4 F 8 and O 2 ), and chamber pressure. Subsequently, the most suitable experimental conditions were identified and used as the central run for analyzing the influence of individual parameters on ICP etching of Ta 2 O 5 . Key findings include the importance of maintaining a 50% C 4 F 8 in total gas flow and trade-offs related to ICP and RF power adjustments. Pressure has a negligible impact on sidewall angle but exerts a more pronounced influence on etch rate and micromasking. A delicate balance among these parameters is crucial for optimal etching results. The recommended recipe (50 W RF platen power, 2000 W ICP power, 10 mTorr pressure, 50% C 4 F 8 in total gas flow) achieves an etch rate of 113.325 nm/min with a smooth and vertical sidewall in PhCs. The entire etching exploration process was conducted on a Ta 2 O 5 layer deposited on a Si substrate. Additionally, this recipe was applied to etch Ta 2 O 5 with a 2 μ m SiO 2 layer interposed between the Ta 2 O 5 layer and the Si substrate, yielding favorable results and preserving the integrity of the PhC sidewall.

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023405_1_6.0004211 - Version of Record
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Accepted/In Press date: 29 January 2025
Published date: 1 March 2025
Additional Information: Publisher Copyright: © 2025 Author(s).

Identifiers

Local EPrints ID: 502086
URI: http://eprints.soton.ac.uk/id/eprint/502086
PURE UUID: add9d61e-834e-4ac2-aa1f-5811e6678160
ORCID for Wenjie Wang: ORCID iD orcid.org/0000-0001-5739-3085

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Date deposited: 16 Jun 2025 16:46
Last modified: 11 Sep 2025 03:19

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Contributors

Author: Wenjie Wang ORCID iD
Author: Libe Arzubiaga Totorika
Author: Maryam Shayesteh
Author: Stephen Stapleton Fenner
Author: Owain Clark
Author: Martin Charlton

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