Effect of extrusion temperature and speed on texture evolution in Mg-Zn-Gd alloy and their correlation with mechanical properties
Effect of extrusion temperature and speed on texture evolution in Mg-Zn-Gd alloy and their correlation with mechanical properties
It is generally believed that the addition of rare earth (RE) elements can modify the texture distribution to form a distinct RE texture, which is typically weaker and more dispersed than conventional textures. In this study, we systematically investigated the influence of extrusion temperature and speed synergy on grain boundary segregation and texture evolution in Mg-2Zn-1Gd (wt.%) alloy. Further investigation using Electron Backscattered Diffraction (EBSD) and Energy Dispersive Spectroscopy (EDS) in Scanning transmission electron microscopy mode (STEM-EDS) revealed that rare earth magnesium alloys (Mg-RE alloys) do not invariably result in the formation of RE textures, that is under low-temperature and low-speed conditions, Zn/Gd co-segregation dominates RE texture formation by increasing the critical strain for dynamic recrystallization and promoting the nucleation of twins and shear bands. Under high-temperature and high-speed conditions, an imbalance in segregation kinetics (grain boundary migration rate > solute diffusion rate) activates basal slip. This basal slip is activated within recrystallized grains to accommodate imposed strain, contributing to the development of a strong basal texture. In addition, the effect of microstructure evolution with extrusion parameters on mechanical properties of Mg-2Zn-1Gd rods are also systematically investigated, and a numerical calculation are conducted to determine the mechanism on the effect of texture evolution on mechanical properties.
Dynamic recrystallization, High-speed extrusion, Mg-RE alloys, Texture
Xu, Shiyuan
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Xu, Jing
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Guan, Bo
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Luo, Xuan
b75c07ad-9dc1-4573-bab9-be974bd464a3
Guan, Dikai
d20c4acc-342a-43fa-a204-7283f0cc33bf
Li, Xuejian
2e031a6e-9a88-4d4d-b6cb-708473a041e9
Yu, Huihui
aab8961e-1ce8-4c34-b8f9-a55ae8eae21a
Wang, Jiahao
858e0fc3-3a66-4dda-b0b8-26337a2ef73e
Hu, Qiang
dcf09eb5-ce60-4171-a799-c4c8eb3e9e33
Xin, Yunchang
f82a1589-22ba-493e-a77b-dbe675477578
30 September 2025
Xu, Shiyuan
bb674f29-cf9f-4131-b776-3d93f60e89e5
Xu, Jing
6f7d4624-efc7-4e88-b260-c39ab19e8090
Guan, Bo
99b14080-fe1c-4e2d-92a2-c9e556d5cb35
Luo, Xuan
b75c07ad-9dc1-4573-bab9-be974bd464a3
Guan, Dikai
d20c4acc-342a-43fa-a204-7283f0cc33bf
Li, Xuejian
2e031a6e-9a88-4d4d-b6cb-708473a041e9
Yu, Huihui
aab8961e-1ce8-4c34-b8f9-a55ae8eae21a
Wang, Jiahao
858e0fc3-3a66-4dda-b0b8-26337a2ef73e
Hu, Qiang
dcf09eb5-ce60-4171-a799-c4c8eb3e9e33
Xin, Yunchang
f82a1589-22ba-493e-a77b-dbe675477578
Xu, Shiyuan, Xu, Jing, Guan, Bo, Luo, Xuan, Guan, Dikai, Li, Xuejian, Yu, Huihui, Wang, Jiahao, Hu, Qiang and Xin, Yunchang
(2025)
Effect of extrusion temperature and speed on texture evolution in Mg-Zn-Gd alloy and their correlation with mechanical properties.
Materials Science and Engineering: A, 947, [149183].
(doi:10.1016/j.msea.2025.149183).
Abstract
It is generally believed that the addition of rare earth (RE) elements can modify the texture distribution to form a distinct RE texture, which is typically weaker and more dispersed than conventional textures. In this study, we systematically investigated the influence of extrusion temperature and speed synergy on grain boundary segregation and texture evolution in Mg-2Zn-1Gd (wt.%) alloy. Further investigation using Electron Backscattered Diffraction (EBSD) and Energy Dispersive Spectroscopy (EDS) in Scanning transmission electron microscopy mode (STEM-EDS) revealed that rare earth magnesium alloys (Mg-RE alloys) do not invariably result in the formation of RE textures, that is under low-temperature and low-speed conditions, Zn/Gd co-segregation dominates RE texture formation by increasing the critical strain for dynamic recrystallization and promoting the nucleation of twins and shear bands. Under high-temperature and high-speed conditions, an imbalance in segregation kinetics (grain boundary migration rate > solute diffusion rate) activates basal slip. This basal slip is activated within recrystallized grains to accommodate imposed strain, contributing to the development of a strong basal texture. In addition, the effect of microstructure evolution with extrusion parameters on mechanical properties of Mg-2Zn-1Gd rods are also systematically investigated, and a numerical calculation are conducted to determine the mechanism on the effect of texture evolution on mechanical properties.
Text
Manuscript-Xu-0710-msea
- Accepted Manuscript
More information
Accepted/In Press date: 26 September 2025
Published date: 30 September 2025
Additional Information:
Publisher Copyright:
© 2025 Elsevier B.V.
Keywords:
Dynamic recrystallization, High-speed extrusion, Mg-RE alloys, Texture
Identifiers
Local EPrints ID: 505977
URI: http://eprints.soton.ac.uk/id/eprint/505977
ISSN: 0921-5093
PURE UUID: a571b7d5-d746-4d84-8ae8-c86921c4f7ad
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Date deposited: 24 Oct 2025 16:50
Last modified: 25 Oct 2025 02:13
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Contributors
Author:
Shiyuan Xu
Author:
Jing Xu
Author:
Bo Guan
Author:
Xuan Luo
Author:
Dikai Guan
Author:
Xuejian Li
Author:
Huihui Yu
Author:
Jiahao Wang
Author:
Qiang Hu
Author:
Yunchang Xin
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