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Sulfate attack testing approaches from concrete to cement paste: a review by RILEM TC 298-EBD

Sulfate attack testing approaches from concrete to cement paste: a review by RILEM TC 298-EBD
Sulfate attack testing approaches from concrete to cement paste: a review by RILEM TC 298-EBD
Most existing test methods determine the sulfate resistance of concrete using accelerated methods in the laboratory, on mortar or concrete specimens. However, these accelerated tests often use high sulfate concentrations or require very complicated setups, which may alter the deterioration mechanisms, while still being laborious and time-consuming. Additionally, the need for more sustainable binders and distinctive properties of systems incorporating emerging supplementary cementitious materials (SCMs) may limit the applicability of conventional test methods. In this context, the Working Group 3 of RILEM TC 298-EBD aims to develop simple accelerated test methods on cement pastes for evaluating sulfate resistance, which directly investigate the reactive component of concrete. Working at this scale can provide reliable results in a much shorter time than traditional tests on mortars and concretes, while providing means to assess the impact of different SCMs and binders on the resistance to sulfate attack. This paper presents our first step, a critical literature review on sulfate deterioration testing from the concrete/mortar to the cement paste scale. We present a general introduction to sulfate attack, common test parameters, assessment methods, test setups for paste specimens, a discussion of potential approaches, and concluding remarks. Insights gained from this review will be instrumental in establishing an effective and reliable approach to sulfate deterioration testing on cement paste specimens.
Cement pastes, Literature review, RILEM TC 298-EBD, Sulfate attack, Supplementary cementitious materials
1359-5997
Wang, Qiao
05bcfc9c-0dd3-4f7b-8e6c-1b6da957be4a
Kunther, Wolfgang
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Li, Ye
86d13351-982d-46c3-9347-22794f647f86
Visalakshi, Talakokula
42d59f92-43b4-4c88-be19-4c0fd45122e4
Gomasa, Ramesh
bb29ab71-aacb-46db-9a54-0fb33657fb81
Amroun, Sofiane
ebce2ec6-c9de-4a7a-933b-a8bbc99a2e7d
De Souza, Diego Jesus
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Kasaniya, Mahipal
8e41a071-03f4-44b2-91c8-769c033599c3
Tole, Ilda
e95b22af-6881-42d6-93c8-13ca06dd56dc
Li, Xuerun
cf021b08-2ba3-4904-b811-609f40404b31
Hooton, R. Douglas
74427db9-ba7c-416a-9cdc-64640dc930ca
Suraneni, Prannoy
05fbf8a2-1933-4bd5-bbde-86113626333c
Wilson, William
06b8e0d9-8f5e-451a-81c3-d376a4a99403
Wang, Qiao
05bcfc9c-0dd3-4f7b-8e6c-1b6da957be4a
Kunther, Wolfgang
31d63762-c597-4e7a-a6a4-aae68cdb03c2
Li, Ye
86d13351-982d-46c3-9347-22794f647f86
Visalakshi, Talakokula
42d59f92-43b4-4c88-be19-4c0fd45122e4
Gomasa, Ramesh
bb29ab71-aacb-46db-9a54-0fb33657fb81
Amroun, Sofiane
ebce2ec6-c9de-4a7a-933b-a8bbc99a2e7d
De Souza, Diego Jesus
d5072eed-9ab7-4b59-9877-1d8b21ed812f
Kasaniya, Mahipal
8e41a071-03f4-44b2-91c8-769c033599c3
Tole, Ilda
e95b22af-6881-42d6-93c8-13ca06dd56dc
Li, Xuerun
cf021b08-2ba3-4904-b811-609f40404b31
Hooton, R. Douglas
74427db9-ba7c-416a-9cdc-64640dc930ca
Suraneni, Prannoy
05fbf8a2-1933-4bd5-bbde-86113626333c
Wilson, William
06b8e0d9-8f5e-451a-81c3-d376a4a99403

Wang, Qiao, Kunther, Wolfgang, Li, Ye, Visalakshi, Talakokula, Gomasa, Ramesh, Amroun, Sofiane, De Souza, Diego Jesus, Kasaniya, Mahipal, Tole, Ilda, Li, Xuerun, Hooton, R. Douglas, Suraneni, Prannoy and Wilson, William (2025) Sulfate attack testing approaches from concrete to cement paste: a review by RILEM TC 298-EBD. Materials and Structures, 58 (7), [232]. (doi:10.1617/s11527-025-02759-x).

Record type: Article

Abstract

Most existing test methods determine the sulfate resistance of concrete using accelerated methods in the laboratory, on mortar or concrete specimens. However, these accelerated tests often use high sulfate concentrations or require very complicated setups, which may alter the deterioration mechanisms, while still being laborious and time-consuming. Additionally, the need for more sustainable binders and distinctive properties of systems incorporating emerging supplementary cementitious materials (SCMs) may limit the applicability of conventional test methods. In this context, the Working Group 3 of RILEM TC 298-EBD aims to develop simple accelerated test methods on cement pastes for evaluating sulfate resistance, which directly investigate the reactive component of concrete. Working at this scale can provide reliable results in a much shorter time than traditional tests on mortars and concretes, while providing means to assess the impact of different SCMs and binders on the resistance to sulfate attack. This paper presents our first step, a critical literature review on sulfate deterioration testing from the concrete/mortar to the cement paste scale. We present a general introduction to sulfate attack, common test parameters, assessment methods, test setups for paste specimens, a discussion of potential approaches, and concluding remarks. Insights gained from this review will be instrumental in establishing an effective and reliable approach to sulfate deterioration testing on cement paste specimens.

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s11527-025-02759-x - Version of Record
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Published date: 24 August 2025
Keywords: Cement pastes, Literature review, RILEM TC 298-EBD, Sulfate attack, Supplementary cementitious materials

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Local EPrints ID: 508573
URI: http://eprints.soton.ac.uk/id/eprint/508573
ISSN: 1359-5997
PURE UUID: bb35055f-868d-4b13-8c5c-c24b0c25515b

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Date deposited: 27 Jan 2026 17:48
Last modified: 28 Jan 2026 04:42

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Contributors

Author: Qiao Wang
Author: Wolfgang Kunther
Author: Ye Li ORCID iD
Author: Talakokula Visalakshi
Author: Ramesh Gomasa
Author: Sofiane Amroun
Author: Diego Jesus De Souza
Author: Mahipal Kasaniya
Author: Ilda Tole
Author: Xuerun Li
Author: R. Douglas Hooton
Author: Prannoy Suraneni
Author: William Wilson

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