Trans-dibromodioxodimethylformamide molybdenum(VI) MoO2Br2(OCHNMe2)(2)
Trans-dibromodioxodimethylformamide molybdenum(VI) MoO2Br2(OCHNMe2)(2)
The molecular structure of Trans-dibromodioxodimethylformamide molybdenum(VI), MoO2Br2(OCHNMe2)2 has been determined. Crystal data: Triclinic, P-1, a = 12.3005(2), b = 15.8763(4), c = 21.1653(6) Å, ? = 71.992(1)°, ? = 88.966(2)°, ? = 89.999(1)°, V = 3930.1(2) Å, Z = 12. Trans-dibromodioxodimethylformamide molybdenum(VI) was obtained by the reaction of sodium molybdate, HBr and dimethylformamide and was characterized by IR, and 1H NMR spectroscopy and elemental analysis.
spectroscopic characterization, complexes, nmr, dimethylformamide, crystal-structures, molybdenum, ethers, x-ray analysis, synthesis, molecular-structure, addition-compounds
421-427
Drake, J.E.
cf5a2c45-a2cb-4361-8b31-f2295e2050b7
Hursthouse, M.B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Light, M.E.
cf57314e-6856-491b-a8d2-2dffc452e161
Kumar, R.
74dee938-14d6-4728-b727-e15fbb5b35b9
Ratnani, R.
5c33e340-5b43-4fae-b43d-c37ae26100ff
2007
Drake, J.E.
cf5a2c45-a2cb-4361-8b31-f2295e2050b7
Hursthouse, M.B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Light, M.E.
cf57314e-6856-491b-a8d2-2dffc452e161
Kumar, R.
74dee938-14d6-4728-b727-e15fbb5b35b9
Ratnani, R.
5c33e340-5b43-4fae-b43d-c37ae26100ff
Drake, J.E., Hursthouse, M.B., Light, M.E., Kumar, R. and Ratnani, R.
(2007)
Trans-dibromodioxodimethylformamide molybdenum(VI) MoO2Br2(OCHNMe2)(2).
Journal of Chemical Crystallography, 37 (6), .
(doi:10.1007/s10870-007-9186-9).
Abstract
The molecular structure of Trans-dibromodioxodimethylformamide molybdenum(VI), MoO2Br2(OCHNMe2)2 has been determined. Crystal data: Triclinic, P-1, a = 12.3005(2), b = 15.8763(4), c = 21.1653(6) Å, ? = 71.992(1)°, ? = 88.966(2)°, ? = 89.999(1)°, V = 3930.1(2) Å, Z = 12. Trans-dibromodioxodimethylformamide molybdenum(VI) was obtained by the reaction of sodium molybdate, HBr and dimethylformamide and was characterized by IR, and 1H NMR spectroscopy and elemental analysis.
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Published date: 2007
Keywords:
spectroscopic characterization, complexes, nmr, dimethylformamide, crystal-structures, molybdenum, ethers, x-ray analysis, synthesis, molecular-structure, addition-compounds
Identifiers
Local EPrints ID: 54286
URI: http://eprints.soton.ac.uk/id/eprint/54286
ISSN: 1074-1542
PURE UUID: 5c32466e-b1dc-4d2c-a34e-a2de157fae25
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Date deposited: 31 Jul 2008
Last modified: 16 Mar 2024 03:04
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Author:
J.E. Drake
Author:
R. Kumar
Author:
R. Ratnani
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