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A catemer-to-dimer structural transformation in cyheptamide

A catemer-to-dimer structural transformation in cyheptamide
A catemer-to-dimer structural transformation in cyheptamide
A catemeric crystal structure of cyheptamide undergoes a transformation in the solid-state upon heating to produce a dimer-based form whose structure has been determined from laboratory X-ray powder diffraction (XRPD) data, thereby providing the first conclusive evidence of a carbamazepine analogue crystallising in both hydrogen bonded motifs.
carbamazepine, molecular-crystal structures, refinement, packing motifs, chlorothiazide, powder diffraction data, 10, collection, 11-dihydrocarbamazepine
1466-8033
26-28
Florence, A.J.K.
05af2713-c875-43fc-9c43-5865423e4845
Gelbrich, T.
42309d69-eaf1-4bb7-ba2e-db61f338e370
Hursthouse, M.B.N.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Johnston, A.
2c3d6549-ffa2-4e7b-9812-91aadc0adee6
Fernandes, P.
fdfcc886-6561-46d9-a1c4-7cfd61ecefd4
Leech, C.K.
b172be32-44b6-4c5c-a54b-e322828dbf69
Florence, A.J.K.
05af2713-c875-43fc-9c43-5865423e4845
Gelbrich, T.
42309d69-eaf1-4bb7-ba2e-db61f338e370
Hursthouse, M.B.N.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Johnston, A.
2c3d6549-ffa2-4e7b-9812-91aadc0adee6
Fernandes, P.
fdfcc886-6561-46d9-a1c4-7cfd61ecefd4
Leech, C.K.
b172be32-44b6-4c5c-a54b-e322828dbf69

Florence, A.J.K., Gelbrich, T., Hursthouse, M.B.N., Johnston, A., Fernandes, P. and Leech, C.K. (2008) A catemer-to-dimer structural transformation in cyheptamide. CrystEngComm, 10 (1), 26-28. (doi:10.1039/b712547j).

Record type: Article

Abstract

A catemeric crystal structure of cyheptamide undergoes a transformation in the solid-state upon heating to produce a dimer-based form whose structure has been determined from laboratory X-ray powder diffraction (XRPD) data, thereby providing the first conclusive evidence of a carbamazepine analogue crystallising in both hydrogen bonded motifs.

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More information

Submitted date: 16 August 2007
Published date: 2008
Keywords: carbamazepine, molecular-crystal structures, refinement, packing motifs, chlorothiazide, powder diffraction data, 10, collection, 11-dihydrocarbamazepine

Identifiers

Local EPrints ID: 54452
URI: http://eprints.soton.ac.uk/id/eprint/54452
ISSN: 1466-8033
PURE UUID: c4b61549-e524-49a4-bc69-10d827d6911e

Catalogue record

Date deposited: 06 Aug 2008
Last modified: 13 Mar 2019 20:38

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