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1,4-Phenylene-bis-(3,4-dichloro-5-phenylcarbamoyl- 1H-pyrrole-2-carboxamide) bis(tetrabutylammonium chloride) acetonitrile disolvate

1,4-Phenylene-bis-(3,4-dichloro-5-phenylcarbamoyl- 1H-pyrrole-2-carboxamide) bis(tetrabutylammonium chloride) acetonitrile disolvate
1,4-Phenylene-bis-(3,4-dichloro-5-phenylcarbamoyl- 1H-pyrrole-2-carboxamide) bis(tetrabutylammonium chloride) acetonitrile disolvate
The title compound, C30H20N6O4Cl4.2C16H36N+·2Cl ·2C2H3N, contains two hydrogen-bonded chloride anions bound to 1,4-phenylene-bis-(3,4-dichloro-5-phenylcarbamoyl-1H-pyrrole-2-carboxamide) as the tetrabutylammonium salt. There is also a short pyrrolic hydrogen bond (NCl = 3.068 (3) Å), and two longer ones to the amino H atoms [NCl = 3.269 (3) Å and 3.275 (3) Å]. The neutral molecule lies on an inversion centre situated at the centre of the central benzene ring.
2056-9890
o1300-o1301
Light, Mark E.
cf57314e-6856-491b-a8d2-2dffc452e161
Gale, Philip A.
c840b7e9-6847-4843-91af-fa0f8563d943
Navakhun, Korakot
cf9bcc17-cf8a-4136-a523-d8f933c47a98
Light, Mark E.
cf57314e-6856-491b-a8d2-2dffc452e161
Gale, Philip A.
c840b7e9-6847-4843-91af-fa0f8563d943
Navakhun, Korakot
cf9bcc17-cf8a-4136-a523-d8f933c47a98

Light, Mark E., Gale, Philip A. and Navakhun, Korakot (2005) 1,4-Phenylene-bis-(3,4-dichloro-5-phenylcarbamoyl- 1H-pyrrole-2-carboxamide) bis(tetrabutylammonium chloride) acetonitrile disolvate. Acta Crystallographica Section E Crystallographic Communications, E61 (5), o1300-o1301. (doi:10.1107/S1600536805010688).

Record type: Article

Abstract

The title compound, C30H20N6O4Cl4.2C16H36N+·2Cl ·2C2H3N, contains two hydrogen-bonded chloride anions bound to 1,4-phenylene-bis-(3,4-dichloro-5-phenylcarbamoyl-1H-pyrrole-2-carboxamide) as the tetrabutylammonium salt. There is also a short pyrrolic hydrogen bond (NCl = 3.068 (3) Å), and two longer ones to the amino H atoms [NCl = 3.269 (3) Å and 3.275 (3) Å]. The neutral molecule lies on an inversion centre situated at the centre of the central benzene ring.

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Published date: 9 April 2005

Identifiers

Local EPrints ID: 15395
URI: http://eprints.soton.ac.uk/id/eprint/15395
ISSN: 2056-9890
PURE UUID: 599a51a7-7a2a-44f0-bc12-23b328d51c6d
ORCID for Mark E. Light: ORCID iD orcid.org/0000-0002-0585-0843
ORCID for Philip A. Gale: ORCID iD orcid.org/0000-0001-9751-4910

Catalogue record

Date deposited: 11 Apr 2005
Last modified: 07 Oct 2020 07:24

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Contributors

Author: Mark E. Light ORCID iD
Author: Philip A. Gale ORCID iD
Author: Korakot Navakhun

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