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Three-dimensional study of grain scale tensile twinning activity in magnesium: a combination of microstructure characterization and mechanical modeling

Three-dimensional study of grain scale tensile twinning activity in magnesium: a combination of microstructure characterization and mechanical modeling
Three-dimensional study of grain scale tensile twinning activity in magnesium: a combination of microstructure characterization and mechanical modeling
Tensile twinning is a main deformation mode in hexagonal close packed structure metals, so it is important to comprehensively understand twinning mechanisms which are not fully disclosed using 2D or small volume 3D characterization techniques. A large area 3D electron backscatter diffraction (EBSD) measurement and crystal plasticity modeling were carried out to investigate the tensile twinning behaviors in a magnesium (Mg) alloy. The results showed that tensile twinning activity was underestimated using conventional 2D EBSD scans. When compressed to yield point, the examined twin frequency with 2D was lower than that using 3D EBSD. The effects of Schmid factor (SF) on twinning were investigated. Almost all high Schmid factor (SF>0.35) grains were twinned. A surprising high twin frequency of 82% in middle SF (0.35>=SF>=0.15) grains was observed, which was unexpected since the middle SF grains were believed to be unfavorable for twinning. The twin frequency in low SF (SF<0.15) grains was slightly increased from 2D to 3D EBSD due to the small volume of twins. The shear stress maintained a high level and was homogeneously distributed in high SF grains, facilitating twin nucleation and growth. The shear stress was distributed heterogeneously within the middle SF grains, and twins were nucleated within areas with positive shear stress. The shear stress in low SF grains was not favorable for twinning and twins occurred in the vicinity of stress accumulation. Twinning activities in the same grain varied on different layers. It was attributed to the stress fluctuation derived from grain environment changes.
3D EBSD, Crystal plasticity modeling, Mg alloy, Micro-mechanics, Schmid factor
1359-6454
Zeng, Xun
ff832409-a044-4a72-af7a-2c89874387f3
Liu, Chuanlai
2ade13d3-ff8f-41bd-b6f6-9b93d403923d
Zhao, Chaoyu
1e18f395-5ea9-48d7-87d9-a7d37869dd5b
Dong, Jie
17878af9-bcd2-4fe2-9959-a2ffbb108d92
Roters, Franz
9905e8c3-d794-41eb-b48d-67a49c502071
Guan, Dikai
d20c4acc-342a-43fa-a204-7283f0cc33bf
Zeng, Xun
ff832409-a044-4a72-af7a-2c89874387f3
Liu, Chuanlai
2ade13d3-ff8f-41bd-b6f6-9b93d403923d
Zhao, Chaoyu
1e18f395-5ea9-48d7-87d9-a7d37869dd5b
Dong, Jie
17878af9-bcd2-4fe2-9959-a2ffbb108d92
Roters, Franz
9905e8c3-d794-41eb-b48d-67a49c502071
Guan, Dikai
d20c4acc-342a-43fa-a204-7283f0cc33bf

Zeng, Xun, Liu, Chuanlai, Zhao, Chaoyu, Dong, Jie, Roters, Franz and Guan, Dikai (2023) Three-dimensional study of grain scale tensile twinning activity in magnesium: a combination of microstructure characterization and mechanical modeling. Acta Materialia, 255, [119043]. (doi:10.1016/j.actamat.2023.119043).

Record type: Article

Abstract

Tensile twinning is a main deformation mode in hexagonal close packed structure metals, so it is important to comprehensively understand twinning mechanisms which are not fully disclosed using 2D or small volume 3D characterization techniques. A large area 3D electron backscatter diffraction (EBSD) measurement and crystal plasticity modeling were carried out to investigate the tensile twinning behaviors in a magnesium (Mg) alloy. The results showed that tensile twinning activity was underestimated using conventional 2D EBSD scans. When compressed to yield point, the examined twin frequency with 2D was lower than that using 3D EBSD. The effects of Schmid factor (SF) on twinning were investigated. Almost all high Schmid factor (SF>0.35) grains were twinned. A surprising high twin frequency of 82% in middle SF (0.35>=SF>=0.15) grains was observed, which was unexpected since the middle SF grains were believed to be unfavorable for twinning. The twin frequency in low SF (SF<0.15) grains was slightly increased from 2D to 3D EBSD due to the small volume of twins. The shear stress maintained a high level and was homogeneously distributed in high SF grains, facilitating twin nucleation and growth. The shear stress was distributed heterogeneously within the middle SF grains, and twins were nucleated within areas with positive shear stress. The shear stress in low SF grains was not favorable for twinning and twins occurred in the vicinity of stress accumulation. Twinning activities in the same grain varied on different layers. It was attributed to the stress fluctuation derived from grain environment changes.

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Accepted/In Press date: 29 May 2023
e-pub ahead of print date: 30 May 2023
Published date: 15 August 2023
Additional Information: Funding Information: This work was supported by the UKRI Future Leaders Fellowship, MR/T019123/2. CL and FR acknowledge financial support by the Deutsche Forschungsgemeinschaft (DFG) within projects A01 and C01 of the Collaborative Research Center (SFB) 1394 “Structural and Chemical Atomic Complexity - from defect phase diagrams to material properties”, project ID 409476157. CZ and JD acknowledge the financial supports of the National Natural Science Foundation of China (Grant no. 52071208). The fruitful discussion with Dr Chaitanya Paramatmuni from University of Sheffield is gratefully acknowledged. Funding Information: This work was supported by the UKRI Future Leaders Fellowship , MR/T019123/2 . CL and FR acknowledge financial support by the Deutsche Forschungsgemeinschaft (DFG) within projects A01 and C01 of the Collaborative Research Center (SFB) 1394 “Structural and Chemical Atomic Complexity - from defect phase diagrams to material properties”, project ID 409476157 . CZ and JD acknowledge the financial supports of the National Natural Science Foundation of China (Grant no. 52071208 ). The fruitful discussion with Dr Chaitanya Paramatmuni from University of Sheffield is gratefully acknowledged. Publisher Copyright: © 2023 The Author(s)
Keywords: 3D EBSD, Crystal plasticity modeling, Mg alloy, Micro-mechanics, Schmid factor

Identifiers

Local EPrints ID: 477898
URI: http://eprints.soton.ac.uk/id/eprint/477898
ISSN: 1359-6454
PURE UUID: e248b68f-8ce3-4c43-8e30-01f493d67cb8
ORCID for Dikai Guan: ORCID iD orcid.org/0000-0002-3953-2878

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Date deposited: 16 Jun 2023 16:31
Last modified: 17 Mar 2024 04:17

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Contributors

Author: Xun Zeng
Author: Chuanlai Liu
Author: Chaoyu Zhao
Author: Jie Dong
Author: Franz Roters
Author: Dikai Guan ORCID iD

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