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Development of a lab-based in situ XCT oven for vacuum-bag processing of prepreg laminates

Development of a lab-based in situ XCT oven for vacuum-bag processing of prepreg laminates
Development of a lab-based in situ XCT oven for vacuum-bag processing of prepreg laminates

Real-time 3D microstructure changes in prepreg laminates during curing was observed using widely available X-ray Computed Tomography (XCT) hardware at high temporal resolution (2 min) and spatial resolution (25 µm voxel size). The methodology was demonstrated in a cylindrical convection oven with an internal diameter of 100 mm, a heating rate of 2°C/min, a maximum operating temperature of 135°C, and an integrated vacuum line. The technique was applied to three representative carbon fibre reinforced epoxy prepreg samples having flat, tapered and corner geometries. The increasingly complex geometries lead to higher void mobility and thickness changes that were captured in 40-50 mm size samples. Image processing of the XCT data was enhanced by the use of deep learning semantic segmentation for feature extraction. Uninterrupted microstructure evolution was visualised in larger samples and more realistic processing conditions than previous lab-based In Situ XCT studies.

consolidation, CT analysis, cure, out of autoclave processing
0021-9983
Galvez-Hernandez, Pedro
cb3fcdc1-6634-43ef-ad01-e3c1cb66b981
Nazemi, Ehsan
d7184499-c6fb-4b10-abff-b8fb5431f69f
Radhakrishnan, Arjun
c0674f84-1b81-43f4-b677-7c7bb7ea5aa3
Alvarez-Borges, Fernando
5512cdfd-6ad3-475f-8aec-2fc767607314
Mavrogordato, Mark
f3e0879b-118a-463a-a130-1c890e9ab547
Sinclair, Ian
6005f6c1-f478-434e-a52d-d310c18ade0d
Kratz, James
c6e20b9a-b72f-4386-b73b-175fba499511
Galvez-Hernandez, Pedro
cb3fcdc1-6634-43ef-ad01-e3c1cb66b981
Nazemi, Ehsan
d7184499-c6fb-4b10-abff-b8fb5431f69f
Radhakrishnan, Arjun
c0674f84-1b81-43f4-b677-7c7bb7ea5aa3
Alvarez-Borges, Fernando
5512cdfd-6ad3-475f-8aec-2fc767607314
Mavrogordato, Mark
f3e0879b-118a-463a-a130-1c890e9ab547
Sinclair, Ian
6005f6c1-f478-434e-a52d-d310c18ade0d
Kratz, James
c6e20b9a-b72f-4386-b73b-175fba499511

Galvez-Hernandez, Pedro, Nazemi, Ehsan, Radhakrishnan, Arjun, Alvarez-Borges, Fernando, Mavrogordato, Mark, Sinclair, Ian and Kratz, James (2024) Development of a lab-based in situ XCT oven for vacuum-bag processing of prepreg laminates. Journal of Composite Materials. (doi:10.1177/00219983241302328).

Record type: Article

Abstract

Real-time 3D microstructure changes in prepreg laminates during curing was observed using widely available X-ray Computed Tomography (XCT) hardware at high temporal resolution (2 min) and spatial resolution (25 µm voxel size). The methodology was demonstrated in a cylindrical convection oven with an internal diameter of 100 mm, a heating rate of 2°C/min, a maximum operating temperature of 135°C, and an integrated vacuum line. The technique was applied to three representative carbon fibre reinforced epoxy prepreg samples having flat, tapered and corner geometries. The increasingly complex geometries lead to higher void mobility and thickness changes that were captured in 40-50 mm size samples. Image processing of the XCT data was enhanced by the use of deep learning semantic segmentation for feature extraction. Uninterrupted microstructure evolution was visualised in larger samples and more realistic processing conditions than previous lab-based In Situ XCT studies.

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galvez-hernandez-et-al-2024-development-of-a-lab-based-in-situ-xct-oven-for-vacuum-bag-processing-of-prepreg-laminates - Version of Record
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e-pub ahead of print date: 27 November 2024
Keywords: consolidation, CT analysis, cure, out of autoclave processing

Identifiers

Local EPrints ID: 497298
URI: http://eprints.soton.ac.uk/id/eprint/497298
ISSN: 0021-9983
PURE UUID: dfa68133-2b94-4df9-8a4e-e85146d9b972
ORCID for Fernando Alvarez-Borges: ORCID iD orcid.org/0000-0002-6940-9918

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Date deposited: 17 Jan 2025 17:50
Last modified: 11 Jul 2025 02:12

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Contributors

Author: Pedro Galvez-Hernandez
Author: Ehsan Nazemi
Author: Arjun Radhakrishnan
Author: Fernando Alvarez-Borges ORCID iD
Author: Ian Sinclair
Author: James Kratz

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